Ultrapure Water Systems

  

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General

      Many industries have become increasingly dependant on Ultrapure Water in processing its products.   Each application has its unique maximum contaminants' level requirement.  For example, among other guidelines, Electronic Grade water for Semiconductor processing requires up to 18.3 mohm resistivity;  and Reagent Grade water for WFI requires less than 10 ppm total solids, TOC limit of 500 ppb, and Bacterial Count less than 100 CFU/ml, followed by Sterilization of the final product.  High purity water is obtained by further processing of the Reverse Osmosis permeate through a Polishing Loop.  Typical equipment required in a polishing loop include Second Stage RO Systems (RO), Ion Exchangers (IE), Electrodeionizers (EDI) and Ultraviolet Disinfection Systems (UV).
 

 

 

 

Polishing Reverse Osmosis Systems

Description

Type

Second stage RO systems

Usage

Polishing of RO permeate to provide superior product water quality

Applications

Ultrapure water

Equipment

Single or multiple-train, depending on system capacity.  Single or double pass, depending on permeate quality requirements.  Typical system consists of three main sections or subsystems; common Pretreatment, Main Treatment consisting of single or multiple-train RO (or UF) subsystem, and a common Post Treatment.

Capacity

 Varies, depending on custom requirements and application

Features

Pretreatment

Customized to condition RO permeate for further membrane treatment.  May include chemical treatment, vacuum degasifier, ultraviolet or softening equipment

Main Treatment

Membrane Separation Systems using high or standard rejection RO membrane elements, (or UF membranes).  Single or double-pass systems, depending on permeate quality requirements. 

Post Treatment 

Customized, for conditioning of the Main Treatment effluent (permeate).  May include chemical treatment, mixed bed demineralization, final filtration and UV sterilization.

Instruments

Locally mounted primary elements. Monitoring and Control Instruments are mounted on the Main Control Panel (MCP)

Controls

PLC controlling the entire plant sections.  Typically located inside the MCP

Advantages

Design

1.  Lower installation cost, less installation time, and easy piping hookup
2.  High corrosion resistance
3.  Consistent permeate quality
4.  Consistent reject quality

Operation

Reliable; lower capital cost

Performance

Product Resistivity exceeding 16 mohm.cm.  Double-pass systems'  permeate meets PW and/or WFI standards.

Components

Pressure Vessels

FRP or Stainless steel

Support Structure

FRP or CS epoxy painted or powder coated, supporting the pressure vessel assemblies

Internals

Corrosion resistant PVC and/ or 316L SS

Piping

1.  Train mounted High Pressure piping: Fabricated of Sch 10 -316L SS, PVDF or Sch 80 PVC
2.  Train mounted Low Pressure piping: Fabricated of Sch 10 -316L SS, PVDF or Sch 80 PVC
3.  Interconnecting piping: Fabricated of PVDF, Sch 80 PVC or CPVC

Valves

1.  Control Valves: Modulating, with Pneumatic or Electrical Actuator
2.  Auto Isolation Valves: Pneumatic or Electrical operator w/ Auto On-Off control
3.  Manual Valves: SS or Plastic, as required

Instruments

Provided for continuous monitoring and control of Flow, Pressure, Temperature, Level and Analytical parameters, such as pH, Conductivity, ORP, Turbidity, TOC, etc.

Controls

Automatic control via Programmable Logic Controller (PLC), mounted inside the Main Control Panel (MCP)

Electrical

Motor Control Center (MCC), including motor starters and controls; Local Starter Panels and Junction Boxes; Miscellaneous hardware

Options

1.  Adjustable Frequency Drive (AFD) for the Medium Pressure Pump (MPP)
2.  Data Acquisition and Monitoring System (DAQM) 

 

 

 

 

Ion Exchangers

Description

Type

Mixed Bed

Usage

Polishing of RO permeate to provide superior product water quality

Applications

Ultrapure water

Equipment

Single vessel containing mixed Cation and Anion resins, in H-OH form.  The unit is self contained with face piping, valves, I&C's mounted on the same skid.  Multiple units can be used in parallel for increased capacities. Resin regeneration is conducted in-place using Caustic and Acid Regenerants

Capacity

 Varies, depending on custom requirements and application

Features

Vessel

Skid mounted.  100% Free Board to allow for efficient backwash.  Top and bottom head Manway for easy inspection. 

Regeneration

Automatic, allowing backwash, rinsing and resin mixing steps during Regeneration.

Instruments

Locally mounted, easy accessed

Controls

PLC for service and regeneration sequencing

Advantages

Design

1.  Lower installation cost, less installation time, and easy piping hookup
2.  High corrosion resistance
3.  Superior flow distribution

Operation

Reliable; lower capital cost

Performance

Product Resistivity exceeding 16 mohm.cm

Components

Vessel

Designed per sec VIII Div 1 ASME code, CS painted, Epoxy or Rubber lined

Support Structure

Structural steel base, painted

Internals

Corrosion resistant PVC and/ or 316L SS

Piping

External, Internal and Interconnecting all Sch 80 PVC or Sch 10 316

Valves

BF Isolation valves, Pneumatic or Electrical operator w/ Auto On-Off control 

Instruments

Sight Glass; In / Out pres. gauge, Inlet flow Indicating Transmitter, Effluent Conductivity Analyzer

Controls

Programmable Logic Controller (PLC), Local or Remote mount

Electrical

Local Control Panel housing 

Options

1.  Differential Pressure Switch, Effluent Na and SiO2 Analyzer, pH monitor
2.  Caustic and Acid injection systems
3.  Single or Duplex Air Blower for resin mixing.  (Required if oil-free plant air is not available)

 

 

 

Electrodeionizers

 

 

 

Description

Type

Electrodeionizer, Modular design E-Cell Stacks

Usage

Polishing of RO permeate to provide superior product water quality

Applications

Ultrapure water

Equipment

Self contained complete integrated systems for Ultrapure water production.  The E-Cell Stack represents the unit building block of the system.

Capacity

Ranges from 25 gpm to 150 gpm

Features

Configuration

The complete system is configured in Stack and Rack arrangement

Operation

Automatic, 

Instruments

Locally mounted

Controls

PLC, with continuous monitoring of process parameters

Advantages

Design

1.  Modular, providing flexibility to accommodate small and large capacities
2.  Lower installation cost, less installation time, and easy piping hookup
3.  Withstands pressure up to 100 psig

Operation

Simple; Short startup time; No regeneration; No chemicals required, Lower operating cost

Performance

Robust; 90-95% Recovery rate; Wide range of feed water quality; Product Resistivity exceeding 16 mohm.cm

Components

E-Cell Stacks

Each E-Cell Stack is capable of producing 12.5 gpm of purified water

Concentrate Pump

Re-circulates the concentrate back into the C chamber inlet.  A percentage of this flow is diverted to the raw water inlet for recovery and a very small portion goes to waste 

Piping

Sch. 80 PVC or Polypropylene

Valves

For Isolation of flow control 

Instruments

Flow Indicator with Switch; Pressure Indicator; Resistivity or Cond. Meter  

Controls

PLC housed in a Local Control Panel (LCP) for monitoring and control of  process parameter and safety shutdown.  The LCP is equipped with MMI

Electrical

Electrical Power Rectifier w/ 0-600 VDC variable voltage, and 0-4.5 Amp variable current.  Rectifier houses the Motor Starter of the Recirc. Pump

Options

Brine Pump, required for systems with low conductivity feed water to maintain suitable concentrate conductivity in the polishing loop

 

 

 

 

UV Systems

 

 

 

Description

Type

Industrial-type Ultraviolet Disinfection Systems 

Usage

Disinfection; Effective control of microorganism contamination
1.  Pre and Post RO, UF and MF Systems
2.  Pre and Post Deionizers
3.  Recirculation Loops

Applications

Seawater desalination, Brackish water systems, High purity water systems

Equipment

Purifier chamber containing UV lamp(s) and internal baffles.  316L SS shell construction with flanged connections.  

System Capacity

Ranges from 50 gpm to 600 gpm

Features

Configuration

LED pilot lights in geometric positioning to match UV chamber lamps.
Internal Baffles to prevent laminar flow, maximize turbulence and microorganism destruction; UV sight or monitor port.  

Operation

No moving parts.  Hard glass type UV lamps rated for over 9,000 hours of continuous use.  Manual quartz sleeve cleaning system

Instruments

Locally mounted running time meter

Controls

NEMA rated power box with heavy duty On-Off switch

Advantages

Design

1.  Modular, providing flexibility to accommodate small and large capacities
2.  Lower installation cost, less installation time, and easy piping hookup
3.  Design pressure of 150 psig and up to 125 psig operating pressure

Operation

Simple; No moving parts; Complete water turbulence and maximum destruction of microorganisms.

Performance

More than 30,000 micro-watt sec/cm2 of 2537 Angstrom wavelength (254 Nanometer) of UV energy across fluid medium for 99.9% kill of contaminating microorganisms

Components

UV Chamber

316 SS, Electro-polished and passivated to MIL Spec S-5002 on both interior and exterior.  Water tight vibration resistant connections

UV Lamps

High intensity hard glass type.  Each UV lamp is protected in a high transmition pure-fused quartz sleeve for peak UV dosage  

Piping

150-lb, 316 SS Flange connections in inlet and outlet

Valves

1/4" Sample ports on inlet and outlet 

Instruments

UV sight or monitor port; Running time meter

Controls

PLC housed in a Local Control Panel (LCP) for monitoring and control of  process parameter and safety shutdown.  The LCP is equipped with MMI

Electrical

NEMA rated power box with heavy duty On-Off switch

Options

1.  PVDF lining
2.  High temperature safety cut-off switch
3.  Narrow band germicidal UV Monitor senses over 90% 2537 A germicidal wavelength.
4.  Automatic timer controlled quartz sleeve cleaning system
5.  100% redundancy with automatic switch-over

 

 

 

 

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                               Last modified: February 05, 2009